Nanoscale partioning of carbon black in styrene butadiene rubber and butadiene rubber miscible blends and its effect on physico-mechanical properties (Record no. 75250)

MARC details
000 -LEADER
fixed length control field 02422nam a22002057a 4500
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Personal name Kaliyathan, A.V.
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Title Nanoscale partioning of carbon black in styrene butadiene rubber and butadiene rubber miscible blends and its effect on physico-mechanical properties
260 ## - PUBLICATION, DISTRIBUTION, ETC. (IMPRINT)
Name of publisher Journal of Rubber Research, 26(2): 2023. 81-98.
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Other physical details May
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Summary, etc Determining the partitioning of carbon black [CB] in miscible rubber–rubber blends [RRB’s] is a demanding problem in the rubber industry, testing one’s ability (especially tyre industry); hence, this research work aims to investigate the partitioning of CB in miscible styrene butadiene rubber [SBR]/butadiene rubber [BR] blends. SBR:BR with blend ratios of 70:30/50:50 and 30:70 with 50 phr CB were prepared on two-roll mill. Nanoscale partitioning of CB within the nanoscale phase-separated SBR/BR blends was quantitatively determined using dynamic mechanical analysis [DMA]. DMA confirmed 63%, 93%, and 45% of CB partitioning towards BR phases of 70:30, 50:50, and 30:70 in CB-filled SBR/BR blends. An attempt to determine the partitioning of CB was also made by making use of solid-state nuclear magnetic resonance spectroscopy [SS-NMR spectroscopy] to interrelate the partitioning of CB determined using DMA. TEM images were helpful in observing CB's dispersion and network ability in CB-filled SBR/BR blends. The results of CB partitioning confirm maximum partitioning of CB towards the nano-dispersed phase in CB-filled SBR/BR blends and are in well agreement with the constrained regions of BR and mechanical properties of CB-filled SBR/BR blends. Attenuated total reflectance-Fourier transform infrared spectroscopy’s (ATR-FTIR spectroscopy) spectra were used as a tool to determine the interactions within CB-filled rubbers and RRB’s in comparison to their neat counterparts. To the best of our knowledge, partitioning of CB controlled by nanoscale phase-separated morphology and its effect on mechanical properties has not been studied so far; hence, this study would be significant to academics and industrial researchers working in the area of rubber composites.
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Topical Term Crosslinking
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Topical Term Blends
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Topical Term Elastomers
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Topical Term Glass transition
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Topical Term Mechanical properties
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Personal name Rane, A.V.
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Personal name Thomas, S.
856 ## - ELECTRONIC LOCATION AND ACCESS
Uniform Resource Identifier https://doi.org/10.1007/s42464-023-00197-4
942 ## - ADDED ENTRY ELEMENTS (KOHA)
Koha item type Journals
Holdings
Withdrawn status Lost status Damaged status Not for loan Home library Current library Date acquired Koha item type
        RRII Library RRII Library 03/05/2024 Journals