Steric exclusion chromatography study of natural rubber films prepared from fresh field latex (Record no. 69315)

MARC details
000 -LEADER
fixed length control field 01475nam a2200217Ia 4500
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Personal name Bonfils F
245 #0 - TITLE STATEMENT
Title Steric exclusion chromatography study of natural rubber films prepared from fresh field latex
260 ## - PUBLICATION, DISTRIBUTION, ETC. (IMPRINT)
Name of publisher Journal of Natural Rubber Research
Year of publication 1995
300 ## - PHYSICAL DESCRIPTION
Number of Pages 143-153
520 ## - SUMMARY, ETC.
Summary, etc Cyclohexane was used to replace tetrahydrofuran (THF) as the elution phase in analysis of natural rubber by steric exclusion chromatography. The films, which were prepared from fresh field latex and dissolved in cyclohexane, had high gel rates up to 50;in some cases and overestimated average molecular weights. These problems were linked to certain hydrophilic non-rubber constituents and more particularly to the crosslinking they seem to bring about under certain conditions. This study showed that these crosslinking, which are not covalent, could be overcome by adding hydroxylamine neutral sulphate to the latex prior to film preparation, or by washing the films in deionised water before dissolving them. Using a mixed solvent, such as a cyclohexane and THF mixture (95/5,;v/v), to dissolve this type of samples also significantly limited the proportion of gel.
650 ## - SUBJECT ADDED ENTRY--TOPICAL TERM
Topical Term Hevea brasiliensis
650 ## - SUBJECT ADDED ENTRY--TOPICAL TERM
Topical Term Latex
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Topical Term Steric exclusion chromatography
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Personal name Allet Don A
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Personal name Koman Achi A
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Personal name Laigneau J C
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Personal name Sainte Beuve J
700 ## - ADDED ENTRY--PERSONAL NAME
Personal name Sylla X
942 ## - ADDED ENTRY ELEMENTS (KOHA)
Koha item type Journals
Holdings
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