Flame-resistance and thermal stability of 1,4-polydienes modified by dialkyl (or aryl) phosphates (Record no. 59452)

MARC details
000 -LEADER
fixed length control field 01576nam a2200181Ia 4500
100 ## - MAIN ENTRY--AUTHOR NAME
Personal name Derouet D
245 #0 - TITLE STATEMENT
Title Flame-resistance and thermal stability of 1,4-polydienes modified by dialkyl (or aryl) phosphates
260 ## - PUBLICATION, DISTRIBUTION, ETC. (IMPRINT)
Name of publisher Journal of Natural Rubber Research
Year of publication 1996
300 ## - PHYSICAL DESCRIPTION
Number of Pages 25-Sep
520 ## - SUMMARY, ETC.
Summary, etc The chemical modification of 1,4-polydienes by dialkyl (or aryl) phosphates was considered in order to improve their flame-resistance. Chemical introduction of phosphorus onto polydienes was carried out by a two-step process : partial epoxidation of unsaturated units and introduction of the dialkyl (or aryl) phosphate using the reactivity of the P-OH acidic bond towards oxirane rings of epoxidised 1,4-polydienes (synthetic polybutadiene, polyisoprene and liquid natural rubber). Incorporation of phosphprus (around 1.1-1.2 weight percent) in crosslinked polydienes is generally sufficient to produce air fire-resistant materials. The best limiting oxygen indices (LOI) are obtained with diphenyl phosphate. Degradation kinetics of modified polydiene networks at moderate temperatures (from 200 C to 400 C) are more and less similar to those of unmodified specimens but the weight losses are weaker after 400 C. The residual masses after 600 C are relatively important compared to the unmodified specimens which are entirely decomposed at this temperatue.
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Topical Term Dialkyl phosphates
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Topical Term Flame-resistance
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Topical Term Thermal stability
700 ## - ADDED ENTRY--PERSONAL NAME
Personal name Brosse J C
700 ## - ADDED ENTRY--PERSONAL NAME
Personal name Morvan F
942 ## - ADDED ENTRY ELEMENTS (KOHA)
Koha item type Journals
Holdings
Withdrawn status Lost status Damaged status Not for loan Home library Current library Shelving location Date acquired Serial Enumeration / chronology Koha item type
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